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BMJ 329 , 553557 (2004)

NMR titration experiments 1 H NMR spectra were recorded on a Bruker 500 MHz spectrometer at 310 K using Bruker Topspin (v.4.1.4) software and analysed using MestRenova (v.5.0.1-35756) or Bruker Topspin (v.4.1.4) software, and chemical shifts are expressed in ppm using the residual non-deuterated solvent signals as an internal standard

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