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Equivalent h hour/s min minute/s HPLC High Performance Liquid Chromatography DIEA/DIPEA N,N-Diisopropylethylamine DBU l,8-Diazabicyclo[5.4.0]undec-7-ene DMAP 4-Dimethyla mi nopyridine TFA Trifluoroacetic acid TIS Triisopropylsilane AC2O Acetic anhydride DMF N,N-Dimethylformamide DMA N,N-Dimethylacetamide DCM Dichloromethane THF Tetrahydrofuran NMP N-Methyl-2-pyrrolidinone MTBE Methyl-tert-butylether DIPE diisopropylether MeOH Methanol HFIP Hexafluoro-2-propanol TBDMS Tert-butyl-dimethyl-silyl DIC N,N'-Diisopropylcarbodiimide DCC N,N'-Dicyclohexylcarbodiimide EDC N-(3-dimethylaminopropyl)-N'-ethylcarbodiinnide HOBt 1-Hydroxybenzotriazole HO At 1-Hydroxy-7-azabenzotriazole NHS N-Hydroxysuccinimide TBTU 0-(Benzotriazol-l-yl)-N,N,N',N'-tetramethyluroniunn tetrafluoroborate HBTU 0-(Benzotriazol-l-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate HATU 2-(7-Aza-lH-benzotriazole-l-yl)-l, 1,3,3- tetramethyluronium hexafluorophosphate PyBOP (Benzotriazol-l-yloxy)tripyrrolidinophosphoniunn hexafluorophosphate OxymaPure Ethyl 2-cyano-2-hydroxyi mi no-acetate Oxyma-B 5-( Hyd roxy i m ino) 1, 3-dimethyl pyrimidine-2, 4, 6- ( lH,3H,5H)-trione TX-100 Triton X-100, also referred to as polyethylene glycol tert-octylphenyl ether Examples Detailed experimental parameters suitable for the preparation of liraglutide and semaglutide according to the present invention are provided by the following examples, which are intended to be illustrative and not limiting of all possible embodiments of the invention

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